6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Base Information

• Chemical Name: 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride
• CAS No.: 1111643-15-2
• Molecular Formula: C₂₅H₂₄N₂O*ClH
• Molecular Weight: 404.939

Synonyms:6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Chemical Property of 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Chemical Property:

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Technology Process of 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

There total 1 articles about 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

3-Benzyloxybenzaldehyde (1700-37-4) + 5-methyltryptamine hydrochloride (1010-95-3) → 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride (1111643-15-2)

Guidance literature:

With acetic acid; at 95 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.05.024

Reference yield: 45.0%

2-(3-bromopropyl)isoindole-1,3-dione (5460-29-7) + 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride (1111643-15-2) → 6-methyl-1-(3-benzyloxyphenyl)-2-(3-phthalimide-propyl)-1,2,3,4-tetrahydro-β-carboline (1236398-05-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 150 ℃; for 10h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.05.024

Reference yield: 41.9%

2-(2-bromoethyl)isoindoline-1,3-dione (574-98-1) + 6-methyl-1-(3-benzyloxyphenyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride (1111643-15-2) → 6-methyl-1-(3-benzyloxyphenyl)-2-(2-phthalimide-ethyl)-1,2,3,4-tetrahydro-β-carboline (1236398-04-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 150 ℃; for 10h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.05.024

upstream raw materials:

3-Benzyloxybenzaldehyde

5-methyltryptamine hydrochloride

Downstream raw materials:

6-methyl-1-(3-benzyloxyphenyl)-2-(2-phthalimide-ethyl)-1,2,3,4-tetrahydro-β-carboline

6-methyl-1-(3-benzyloxyphenyl)-2-(3-phthalimide-propyl)-1,2,3,4-tetrahydro-β-carboline

6-methyl-1-(3-benzyloxyphenyl)-2-(4-phthalimide-butyl)-1,2,3,4-tetrahydro-β-carboline

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