N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

Base Information

Chemical Name:N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)
CAS No.:1417914-64-7
Molecular Formula:C₃₂H₃₆N₂O₄S₄
Molecular Weight:640.913
Hs Code.:

Synonyms:N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

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Chemical Property of N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

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Technology Process of N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

There total 5 articles about N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 39098-97-0
2-thienylacetic acid chloride

: 1417914-66-9
2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)diethanamine

: 1417914-64-7
N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1007/s00044-012-0410-6

Reference yield:

: 73429-10-4
diethyl 2,2'-(biphenyl-2,2'-diylbis(oxy))diacetate

: 1417914-64-7
N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

2: triethylamine / dichloromethane / 2 h / 0 - 5 °C

3: lithium bromide / tetrahydrofuran / 4 h / 20 °C

4: sodium methylate / tetrahydrofuran / 4 h / 20 °C

5: triethylamine / dichloromethane / 3 h / 20 °C

With lithium aluminium tetrahydride; sodium methylate; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane;
DOI:10.1007/s00044-012-0410-6

Reference yield:

: 1806-29-7
2,2'-dihydroxybiphenyl

: 1417914-64-7
N,N'-(2,2'-(2,2'-(biphenyl-2,2'-diylbis(oxy))bis(ethane-2,1-diyl))bis(sulfanediyl)bis(ethane-2,1-diyl))bis(2-(thiophen-2-yl)acetamide)

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; potassium iodide / acetonitrile / 8 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

3: triethylamine / dichloromethane / 2 h / 0 - 5 °C

4: lithium bromide / tetrahydrofuran / 4 h / 20 °C

5: sodium methylate / tetrahydrofuran / 4 h / 20 °C

6: triethylamine / dichloromethane / 3 h / 20 °C

With lithium aluminium tetrahydride; sodium methylate; potassium carbonate; triethylamine; potassium iodide; lithium bromide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1007/s00044-012-0410-6