5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.0^3,12.0^8,11>dodecan

Base Information

• Chemical Name: 5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.0^3,12.0^8,11>dodecan
• CAS No.: 92447-57-9
• Molecular Formula: C₃₈H₄₀N₂O₄
• Molecular Weight: 588.747

Synonyms:5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.0^3,12.0^8,11>dodecan

Chemical Property of 5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.0^3,12.0^8,11>dodecan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.0^3,12.0^8,11>dodecan

There total 3 articles about 5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.0^3,12.0^8,11>dodecan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-tert-Butyl<(5-tert-butyl-1,3,7,8-tetraphenyl-2,4,9-trioxa-5-azatricyclo<4.2.1.03,7>non-8-yl)methylen>amin-N-oxid (92447-56-8,96392-20-0,116497-20-2) → 5,10-Di-tert-butyl-3,8,11,12-tetraphenyl-2,4,7,9-tetraoxa-5,10-diazatetracyclo<4.4.2.03,12.08,11>dodecan (92447-57-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; for 16h; Ambient temperature; further conditions: MeOH, conc. HCl, r.t., 1 h; MeOH, 3 h , reflux;

Reference yield: 36.0%

C38H40N2O4 (92447-56-8,96392-20-0,116497-20-2) → ((3R,6R)-6-Benzoyl-1,4-di-tert-butyl-3,6-diphenyl-tetrahydro-isoxazolo[4,3-c]isoxazol-3-yl)-phenyl-methanone + (3aS,6aS,6bR,6cR)-2,5-Di-tert-butyl-3a,6a,6b,6c-tetraphenyl-octahydro-1,3,4,6-tetraoxa-2,5-diaza-dicyclopenta[cd,gh]pentalene (92447-57-9)

Guidance literature:

In benzene; at 80 ℃; for 20h; Product distribution; other trimer from vinyl nitroxides;

DOI:10.1021/jo00256a017

Reference yield:

C38H40N2O4 (92447-56-8,96392-20-0,116497-20-2) → 1,2-diphenyl-3-(tert-butylimino)-2-propen-1-one (116376-07-9) + C19H20NO2 (92447-55-7) + ((3R,6R)-6-Benzoyl-1,4-di-tert-butyl-3,6-diphenyl-tetrahydro-isoxazolo[4,3-c]isoxazol-3-yl)-phenyl-methanone + (3aS,6aS,6bR,6cR)-2,5-Di-tert-butyl-3a,6a,6b,6c-tetraphenyl-octahydro-1,3,4,6-tetraoxa-2,5-diaza-dicyclopenta[cd,gh]pentalene (92447-57-9)

Guidance literature:

In tetrahydrofuran; at 49 ℃; Equilibrium constant; Thermodynamic data; ΔG;

DOI:10.1021/jo00256a017

upstream raw materials:

C₃₈H₄₀N₂O₄

N-tert-Butyl<(5-tert-butyl-1,3,7,8-tetraphenyl-2,4,9-trioxa-5-azatricyclo<4.2.1.0^3,7>non-8-yl)methylen>amin-N-oxid

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