Dihydrocarveol-tosylat

Base Information

• Chemical Name: Dihydrocarveol-tosylat
• CAS No.: 640296-42-0
• Molecular Formula: C₁₇H₂₄O₃S
• Molecular Weight: 308.442
• Mol file: 640296-42-0.mol

Synonyms:Dihydrocarveol-tosylat

Chemical Property of Dihydrocarveol-tosylat

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Dihydrocarveol-tosylat

There total 1 articles about Dihydrocarveol-tosylat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,2R,4R)-dihydrocarveol (619-01-2,18675-33-7,18675-34-8,18675-35-9,20549-48-8,22567-21-1,22567-22-2,36237-64-6,38049-26-2,51773-45-6,53796-77-3,53796-80-8,73804-29-2,20549-47-7,17699-09-1) + p-toluenesulfonyl chloride (98-59-9) → Dihydrocarveol-tosylat (640296-42-0)

Guidance literature:

With pyridine;

DOI:10.1021/acs.jafc.6b01645

Reference yield:

Dihydrocarveol-tosylat (640296-42-0) → (1R,2S,4R)-8-p-menthene-2-thiol

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide

2: lithium aluminium tetrahydride / diethyl ether

With lithium aluminium tetrahydride; In diethyl ether; N,N-dimethyl-formamide;

DOI:10.1021/acs.jafc.6b01645

Reference yield:

Dihydrocarveol-tosylat (640296-42-0) + potassium thioacetate (10387-40-3) → C12H20OS

Guidance literature:

In N,N-dimethyl-formamide;

DOI:10.1021/acs.jafc.6b01645

upstream raw materials:

(1R,2R,4R)-dihydrocarveol

p-toluenesulfonyl chloride