methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

Base Information

Chemical Name:methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride
CAS No.:808769-19-9
Molecular Formula:C₁₉H₂₃NO₂*ClH
Molecular Weight:333.858
Hs Code.:

Synonyms:methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

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Chemical Property of methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

Chemical Property:

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Technology Process of methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

There total 4 articles about methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 74998-19-9
methyl 3-(2-oxopropyl)benzoate

: 808769-19-9
methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

Guidance literature:: (R)-1-phenyl-ethyl-amine; methyl 3-(2-oxopropyl)benzoate; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃; for 18h;

With water; sodium hydrogencarbonate; In dichloromethane;

With hydrogenchloride; In methanol;

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 74998-19-9
methyl 3-(2-oxopropyl)benzoate

: 808769-19-9
methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

: methyl [3-((2S)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

Guidance literature:: (R)-1-phenyl-ethyl-amine; methyl 3-(2-oxopropyl)benzoate; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃; for 18h;

With sodium hydrogencarbonate; In dichloromethane; water;

With hydrogenchloride; In methanol;

Reference yield:

: 618-89-3
methyl 3-bromobenzoate

: 808769-19-9
methyl [3-((2R)-2-{[(1R)-1-phenyl-ethyl]-amino}-propyl)-phenyl]-acetate hyrdrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: tributyltin methoxide; tris-(o-tolyl)phosphine / palladium diacetate / toluene / 18 h / 100 °C

1.2: 2 h

2.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 18 h / 20 °C

With tributyltin methoxide; sodium tris(acetoxy)borohydride; acetic acid; tris-(o-tolyl)phosphine; palladium diacetate; In dichloromethane; toluene;