(2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

Base Information

Chemical Name:(2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate
CAS No.:1104072-15-2
Molecular Formula:C₂₂H₃₄F₃NO₅Si
Molecular Weight:477.596
Hs Code.:

Synonyms:(2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

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Chemical Property of (2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

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Technology Process of (2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

There total 1 articles about (2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1104072-13-0
(2S,3S)-methyl 2-amino-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1104072-15-2
(2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

Guidance literature:: With sodium carbonate; In tetrahydrofuran; at 20 ℃;

Reference yield: 100.0%

: 1104072-15-2
(2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

: 1236030-91-3
(2S,3S)-2-(tert-butoxycarbonyl)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoic acid

Guidance literature:: With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 20 ℃; for 16h;

Reference yield: 73.0%

: 1104072-15-2
(2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate

: 1104072-16-3
tert-butyl (1S,2R)-1-(tert-butyldimethylsilyloxy)-3-hydroxy-1-(4-(trifluoromethyl)phenyl)propan-2-ylcarbamate

Guidance literature:: (2S,3S)-methyl 2-(tert-butoxycarbonylamino)-3-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)propanoate; With lithium borohydride; In tetrahydrofuran; ethanol; at 0 - 20 ℃; for 25h;

With water; citric acid; In tetrahydrofuran; ethanol;