C₁₇H₁₈N₄O₄S

Base Information

Chemical Name:C₁₇H₁₈N₄O₄S
CAS No.:112373-38-3
Molecular Formula:C₁₇H₁₈N₄O₄S
Molecular Weight:374.42
Hs Code.:

C<sub>17</sub>H<sub>18</sub>N<sub>4</sub>O<sub>4</sub>S

Synonyms:C₁₇H₁₈N₄O₄S

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Chemical Property of C₁₇H₁₈N₄O₄S

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Technology Process of C₁₇H₁₈N₄O₄S

There total 9 articles about C₁₇H₁₈N₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 112373-37-2
4-Methoxy-1H,1'H-[2,2']bipyrrolyl-5-carboxylic acid hydrazide

: 98-59-9
p-toluenesulfonyl chloride

: 112373-38-3
C₁₇H₁₈N₄O₄S

Guidance literature:: With pyridine; at 25 ℃; for 0.25h;
DOI:10.1016/S0040-4039(00)95451-0 DOI:10.1021/jo00242a013

Reference yield:

: 112373-16-7
4,5-diiodo-3-methoxy-2-(methoxycarbonyl)pyrrole

: 112373-38-3
C₁₇H₁₈N₄O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / H₂, K₂CO₃ / Pd/C / methanol / 3 h / 25 °C

2: 1.) NaH / 1.) THF, 65 deg C, 14 h, 2.) THF, 25 deg C, 15 min

3: 96 percent / polymer-supported Pd(II) acetate / acetic acid / 80 °C / var. reag.: Pd(OAc)2 in CH₃COOH, Pd(OOCCF₃)2 in CF₃COOH

4: 88 percent / LiOCH₃ / methanol / 0.08 h / 25 °C

5: 98 percent / NH₂NH₂ / 4 h / 25 °C

6: 97 percent / pyridine / 0.25 h / 25 °C

With pyridine; polymer-supported Pd(II) acetate; lithium methanolate; hydrogen; sodium hydride; potassium carbonate; hydrazine; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1016/S0040-4039(00)95451-0

Reference yield:

: 112373-18-9
3-methoxy-2-(methoxycarbonyl)-1,1'-carbonyldipyrrole

: 112373-38-3
C₁₇H₁₈N₄O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / polymer bound palladium acetate (2.79percent Pd) / acetic acid / 12 h / 80 °C

2: 88 percent / lithium methoxide / methanol / 0.08 h / 25 °C

3: 98 percent / hydrazine / 4 h / 25 °C

4: 97 percent / pyridine / 0.25 h / 25 °C

With pyridine; polymer bound palladium acetate (2.79percent Pd); lithium methanolate; hydrazine; In methanol; acetic acid;
DOI:10.1021/jo00242a013