3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ⁵-phosphanylidene)-propionamide

Base Information

• Chemical Name: 3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ⁵-phosphanylidene)-propionamide
• CAS No.: 73334-63-1
• Molecular Formula: C₃₀H₂₄Cl₄NO₃P
• Molecular Weight: 619.311
• Mol file: 73334-63-1.mol

Synonyms:3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ⁵-phosphanylidene)-propionamide

Chemical Property of 3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ⁵-phosphanylidene)-propionamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ⁵-phosphanylidene)-propionamide

There total 1 articles about 3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ⁵-phosphanylidene)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,2,2,2-tetrachloro-1-isocyanato-ethane (15145-29-6) + (4-methoxyphenacylidene)triphenyl phosphorane (1777-55-5) → 3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ5-phosphanylidene)-propionamide (73334-63-1)

Guidance literature:

In tetrachloromethane; for 1h; Heating;

DOI:10.1007/BF00765607

Reference yield: 90.0%

3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ5-phosphanylidene)-propionamide (73334-63-1) → [1-Bromo-2-(4-methoxy-phenyl)-2-oxo-1-(1,2,2,2-tetrachloro-ethylcarbamoyl)-ethyl]-triphenyl-phosphonium; bromide

Guidance literature:

With bromine; In chloroform;

DOI:10.1007/BF00765607

Reference yield: 85.0%

3-(4-Methoxy-phenyl)-3-oxo-N-(1,2,2,2-tetrachloro-ethyl)-2-(triphenyl-λ5-phosphanylidene)-propionamide (73334-63-1) → [2-(4-Methoxy-phenyl)-2-oxo-1-(1,2,2,2-tetrachloro-ethylcarbamoyl)-ethyl]-triphenyl-phosphonium; chloride

Guidance literature:

With hydrogenchloride; In chloroform;

DOI:10.1007/BF00765607

upstream raw materials:

1,2,2,2-tetrachloro-1-isocyanato-ethane

(4-methoxyphenacylidene)triphenyl phosphorane