(2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine

Base Information

• Chemical Name: (2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine
• CAS No.: 1067621-62-8
• Molecular Formula: C₁₇H₁₅N₇O₂S
• Molecular Weight: 381.418

Synonyms:(2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine

Chemical Property of (2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine

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Technology Process of (2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine

There total 1 articles about (2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-(2-methylsulfanyl-pyrimidin-4-yl)-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidine-5-yl)-amine (872058-79-2) → (2-methanesulfinyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine (881206-57-1) + (2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine (1067621-62-8)

Guidance literature:

With urea hydrogen peroxide adduct; trifluoroacetic anhydride; In acetonitrile; trifluoroacetic acid; at 0 ℃; for 1h;

Reference yield:

(2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine (1067621-62-8) + 1-(tert-butoxycarbonyl)-4-aminopiperidine (87120-72-7) → 4-{4-[methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amino]-pyrimidin-2-ylamino}-piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:

In 1-methyl-pyrrolidin-2-one; at 100 ℃;

Reference yield:

(2-methanesulfinyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine (881206-57-1) + (2-methanesulfonyl-pyrimidin-4-yl)-methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)-amine (1067621-62-8) + [(3)-(2-amino-propyl)-phenyl]-methanol (861839-97-6) → [3-(2-{4-[methyl-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidine-5-yl)-amino]-pyrimidin-2-ylamino}-propyl)-phenyl]-methanol

Guidance literature:

In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 18h;

upstream raw materials:

methyl-(2-methylsulfanyl-pyrimidin-4-yl)-(7-phenyl-[1,2,4]triazolo[1,5-c]pyrimidine-5-yl)-amine

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