2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

Base Information

Chemical Name:2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide
CAS No.:121215-76-7
Molecular Formula:C₂₁H₁₉Br₂NO₈S₃
Molecular Weight:669.39
Hs Code.:

Synonyms:2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

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Chemical Property of 2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

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Technology Process of 2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

There total 3 articles about 2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 121215-72-3
1,1,3,3-Tetraoxo-5-phenyl-2-phenylthiocarbamoyl-1λ⁶,3λ⁶-[1,3]dithiane-4,6-dicarboxylic acid dimethyl ester

: 121215-76-7
2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

Guidance literature:: With bromine; potassium bromide; In methanol; water; at 50 - 60 ℃;

Reference yield:

: 80934-80-1
5-phenyl-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

: 121215-76-7
2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / (CH₃)3CONa / 2-methyl-propan-2-ol; acetonitrile / 2 h / 20 °C

2: 58 percent / KBr, Br₂ / H₂O; methanol / 50 - 60 °C

With bromine; potassium bromide; sodium t-butanolate; In methanol; water; acetonitrile; tert-butyl alcohol;

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 121215-76-7
2-phenylthiocarbamoyl-5-phenyl-4,6-dibromo-4,6-bis(methoxycarbonyl)-1,3-dithiane 1,1,3,3-tetroxide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / (CH₃)3CONa / 2-methyl-propan-2-ol; acetonitrile / 2 h / 20 °C

2: 58 percent / KBr, Br₂ / H₂O; methanol / 50 - 60 °C

With bromine; potassium bromide; sodium t-butanolate; In methanol; water; acetonitrile; tert-butyl alcohol;