methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

Base Information

Chemical Name:methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside
CAS No.:100639-08-5
Molecular Formula:C₂₈H₃₄O₁₀
Molecular Weight:530.572
Hs Code.:

Synonyms:methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

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Technology Process of methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

There total 3 articles about methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 100639-05-2
(1R,2S,4R,5R,6R)-2,4-Bis-benzyloxymethyl-2-methoxy-3,7-dioxa-bicyclo[4.1.0]heptan-5-ol

: 100639-08-5
methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

Guidance literature:: With barium dihydroxide; In 1,4-dioxane; water; for 168h; Heating;
DOI:10.1016/S0008-6215(00)90756-0

Reference yield:

: 100638-99-1,100639-00-7
2,6-Bis-benzyloxymethyl-6-methoxy-6H-pyran-3-one

: 100639-08-5
methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / sodium borohydride / tetrahydrofuran; H₂O / 0.5 h / Ambient temperature

2: 62 percent / CH₂Cl₂ / 96 h

3: 63 percent / barium hydroxide / H₂O; dioxane / 168 h / Heating

With barium dihydroxide; sodium tetrahydroborate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1016/S0008-6215(00)90756-0

Reference yield:

: 62130-93-2,62130-94-3,100639-03-0
methyl 1,7-di-O-benzyl-3,4-dideoxy-α-DL-erythro-hept-3-en-2-ulopyranoside

: 100639-08-5
methyl 3,4,5-tri-O-acetyl-1,7-di-O-benzyl-α-DL-gluco-hept-2-ulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / CH₂Cl₂ / 96 h

2: 63 percent / barium hydroxide / H₂O; dioxane / 168 h / Heating

With barium dihydroxide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1016/S0008-6215(00)90756-0