5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

Base Information

Chemical Name:5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole
CAS No.:936080-17-0
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

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Chemical Property of 5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

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Technology Process of 5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

There total 1 articles about 5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 607-91-0
myristicin

: 38435-51-7
N-hydroxy-4-methoxy-benzenecarboximidoyl chloride

: 936080-17-0
5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 17h;
DOI:10.1021/acs.jnatprod.5b01007

Reference yield: 69.0%

: 936080-17-0
5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

: 3-hydroxy-4-(7-methoxy-1,3-benzodioxol-5-yl)-1-(4-methoxyphenyl)-1-butanone

Guidance literature:: With hydrogen; boric acid; In methanol; water; at 20 ℃; for 48h; under 760.051 Torr;
DOI:10.1021/acs.jnatprod.5b01007

Reference yield:

: 936080-17-0
5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole

: 4-(7-methoxy-1,3-benzodioxol-5-yl)-1-(4-methoxyphenyl)-1,3-butanediol

Guidance literature:: Multi-step reaction with 2 steps

1: boric acid; hydrogen / methanol; water / 48 h / 20 °C / 760.05 Torr

2: sodium tetrahydroborate / methanol / 1 h / 20 °C

With sodium tetrahydroborate; hydrogen; boric acid; In methanol; water;
DOI:10.1021/acs.jnatprod.5b01007