N'-(Cholestan-3-ylidene)-4-methylbenzene-1-sulfonohydrazide

Base Information

• Chemical Name: N'-(Cholestan-3-ylidene)-4-methylbenzene-1-sulfonohydrazide
• CAS No.: 37826-48-5
• Molecular Formula: C34H54N2O2S
• Molecular Weight: 554.881
• DSSTox Substance ID: DTXSID60958856
• Mol file: 37826-48-5.mol

Synonyms:DTXSID60958856;37826-48-5;N'-(Cholestan-3-ylidene)-4-methylbenzene-1-sulfonohydrazide

Chemical Property of N'-(Cholestan-3-ylidene)-4-methylbenzene-1-sulfonohydrazide

Chemical Property:

• XLogP3: 10.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 8
• Exact Mass: 554.39060014
• Heavy Atom Count: 39
• Complexity: 978

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)NN=C2CCC3(C(C2)CCC4C3CCC5(C4CCC5C(C)CCCC(C)C)C)C

Technology Process of N'-(Cholestan-3-ylidene)-4-methylbenzene-1-sulfonohydrazide

There total 1 articles about N'-(Cholestan-3-ylidene)-4-methylbenzene-1-sulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cholestan-3-one (15600-08-5) + toluene-4-sulfonic acid hydrazide (1576-35-8) → Cholestan-3-on-monotosylhydrazon (37826-48-5)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 72h;

DOI:10.1021/jacs.7b05161

Reference yield: 95.0%

Cholestan-3-on-monotosylhydrazon (37826-48-5) → cholestan-3-one (15600-08-5)

Guidance literature:

Envirocat EPZG; In water; acetone; at 80 ℃; for 4h;

DOI:10.1055/s-1997-5749

Reference yield: 70.0%

p-toluene-sulphonyl-hydrazone of cholestanone (26430-35-3,37826-48-5,105615-82-5) → cholestane (481-20-9,481-21-0,14982-53-7,25269-18-5,40071-70-3,41083-75-4,55123-81-4,55123-82-5,55176-78-8,67069-18-5,69483-40-5,69483-41-6,69483-42-7,69483-43-8,69483-44-9,69483-45-0,69483-46-1,69483-47-2,69483-48-3,74957-94-1,75023-02-8,101834-34-8,101834-35-9,105307-57-1,105307-58-2,105308-41-6)

Guidance literature:

With tetrahydrogenoboratebis(triphenylphosphine)copper(I); In chloroform; for 2h; Heating;

DOI:10.1016/S0040-4039(00)92863-6

upstream raw materials:

cholestan-3-one

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

Cholestan-3-on-N_.N-ditosylhydrazon

cholestan-3-one

cholestane