4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

Base Information

Chemical Name:4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate
CAS No.:225508-13-4
Molecular Formula:C₃₇H₄₄I₄O₆
Molecular Weight:1092.37
Hs Code.:

Synonyms:4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

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Chemical Property of 4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

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Technology Process of 4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

There total 4 articles about 4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 6-(4-tert-butyl-2,6-diiodo-phenoxy)-hexanoic acid

: 225508-10-1
3-(4-tert-Butyl-2,6-diiodophenoxy)propyl 4-hydroxymethylbenzoate

: 225508-13-4
4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1002/(SICI)1521-3765(19990604)5:6<1686::AID-CHEM1686>3.0.CO;2-0

Reference yield:

: 104292-83-3
4-<(tert-butyldimethylsiloxy)methyl>benzoic acid

: 225508-13-4
4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / PPh₃; DEAD / tetrahydrofuran / 20 °C

2: 87 percent / H₂O; TBAF / tetrahydrofuran / 3 h / 20 °C

3: 86 percent / PPh₃; DEAD / tetrahydrofuran

With tetrabutyl ammonium fluoride; water; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1: Substitution / 2: Hydrolysis / 3: Esterification;
DOI:10.1002/(SICI)1521-3765(19990604)5:6<1686::AID-CHEM1686>3.0.CO;2-0

Reference yield:

: 3-(4-tert-butyl-2,6-diiodo-phenoxy)-propan-1-ol

: 225508-13-4
4-{Carboxy[3-(4-tert-butyl-2,6-diiodophenoxy)propyl]phenyl}methyl 6-(4-tert-butyl-2,6-diiodophenoxy)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / PPh₃; DEAD / tetrahydrofuran / 20 °C

2: 87 percent / H₂O; TBAF / tetrahydrofuran / 3 h / 20 °C

3: 86 percent / PPh₃; DEAD / tetrahydrofuran

With tetrabutyl ammonium fluoride; water; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1: Substitution / 2: Hydrolysis / 3: Esterification;
DOI:10.1002/(SICI)1521-3765(19990604)5:6<1686::AID-CHEM1686>3.0.CO;2-0