((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)][B(C₆H₃(CF₃)2)4]

Base Information

• Chemical Name: ((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)][B(C₆H₃(CF₃)2)4]
• CAS No.: 476152-98-4
• Molecular Formula: C₃₁H₆₁OP₂Pt*C₃₂H₁₂BF₂₄
• Molecular Weight: 1570.07

Synonyms:((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)][B(C₆H₃(CF₃)2)4]

Chemical Property of ((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)][B(C₆H₃(CF₃)2)4]

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Technology Process of ((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)][B(C₆H₃(CF₃)2)4]

There total 1 articles about ((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[((C₆H₁₁)2PCH₂)2Pt(CH₃)(O(C₂H₅)2)][B(C₆H₃(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex + [Pt((C6H11)2P)2C2H4(CH3)2] (126949-41-5) → ((C6H11)2PCH2)2Pt(CH3)(O(C2H5)2)(1+)*B(C6H3(CF3)2)4(1-)=[((C6H11)2PCH2)2Pt(CH3)(O(C2H5)2)][B(C6H3(CF3)2)4] (476152-98-4)

Guidance literature:

In diethyl ether; byproducts: CH4; under He atm. using Schlenk techniques; to stirred soln. of (H(OEt2)2B(C6H3(CF3)2)4 in Et2O at room temp. added Pt-complex as solid; vol. reduced; hexane added; placed in a freezer at -30°C for 1 d;filtrate decanted off; washed (hexane); dried (vac.); elem. anal.;

DOI:10.1021/ja020798h

Reference yield: 98.0%

((C6H11)2PCH2)2Pt(CH3)(O(C2H5)2)(1+)*B(C6H3(CF3)2)4(1-)=[((C6H11)2PCH2)2Pt(CH3)(O(C2H5)2)][B(C6H3(CF3)2)4] (476152-98-4) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → [[((C6H11)2PCH2)2Pt]2(μ-biphenyl)][B(C6H3(CF3)2)4]2

Guidance literature:

In benzene; byproducts: CH4; under He atm. using Schlenk techniques; Pt complex suspended in benzene and heated to 80°C for 5 min (alternatively at 25°C for 4 h); soln. cooled to room temp.; solvent decanted off; oil washed (benzene); dried (vac.); dissolved (CH2Cl2); layered (hexane); crystals were obtained; elem. anal.;

DOI:10.1021/ja020798h

Reference yield: 92.0%

((C6H11)2PCH2)2Pt(CH3)(O(C2H5)2)(1+)*B(C6H3(CF3)2)4(1-)=[((C6H11)2PCH2)2Pt(CH3)(O(C2H5)2)][B(C6H3(CF3)2)4] (476152-98-4) + water (7732-18-5) → [((C6H11)2PCH2)2Pt(μ-OH)]2[B(C6H3(CF3)2)4]2

Guidance literature:

In fluorobenzene; byproducts: CH4; under He atm. using Schlenk techniques; Pt complex dissolved in C6H5F; H2O aded with stirring; mixt. stirred at room temp. for 2 h; ppt. collected; washed (benzene); dried (vac.); elem. anal.;

DOI:10.1021/ja020798h

upstream raw materials:

[Pt((C₆H₁₁)2P)2C₂H₄(CH₃)2]

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