C₄₆H₇₇N₃O₁₂Si

Base Information

Chemical Name:C₄₆H₇₇N₃O₁₂Si
CAS No.:1581740-80-8
Molecular Formula:C₄₆H₇₇N₃O₁₂Si
Molecular Weight:892.216
Hs Code.:

C<sub>46</sub>H<sub>77</sub>N<sub>3</sub>O<sub>12</sub>Si

Synonyms:C₄₆H₇₇N₃O₁₂Si

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Chemical Property of C₄₆H₇₇N₃O₁₂Si

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Technology Process of C₄₆H₇₇N₃O₁₂Si

There total 10 articles about C₄₆H₇₇N₃O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1581740-67-1
C₃₄H₅₇N₃O₈Si

: 1581740-80-8
C₄₆H₇₇N₃O₁₂Si

Guidance literature:: With triethylamine; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

Reference yield:

: ((S)-5-Amino-1-carbamoyl-pentyl)-carbamic acid benzyl ester; hydrochloride

: 1581740-80-8
C₄₆H₇₇N₃O₁₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 0.17 h

2.1: triethylamine; trifluoroacetic anhydride / tetrahydrofuran / 0.17 h / 0 - 20 °C

3.1: 10% palladium hydroxide on charcoal; hydrogen; hydrazine hydrate / methanol / 0.17 h / 0 - 20 °C / Reflux

4.1: triethylamine; magnesium sulfate / dichloromethane / 1.5 h / 20 °C

4.3: 0 - 20 °C

5.1: triethylamine; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C

With dmap; 10% palladium hydroxide on charcoal; hydrogen; magnesium sulfate; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; potassium iodide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 80149-80-0
2-(Trimethylsilyl)ethyl 4-nitrophenyl carbonate

: 1581740-80-8
C₄₆H₇₇N₃O₁₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 0.17 h

2.1: triethylamine; trifluoroacetic anhydride / tetrahydrofuran / 0.17 h / 0 - 20 °C

3.1: 10% palladium hydroxide on charcoal; hydrogen; hydrazine hydrate / methanol / 0.17 h / 0 - 20 °C / Reflux

4.1: triethylamine; magnesium sulfate / dichloromethane / 1.5 h / 20 °C

4.3: 0 - 20 °C

5.1: triethylamine; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C

With dmap; 10% palladium hydroxide on charcoal; hydrogen; magnesium sulfate; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; potassium iodide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;