{Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine

Base Information

Chemical Name:{Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine
CAS No.:122214-22-6
Molecular Formula:C₁₄H₂₇NSi
Molecular Weight:237.461
Hs Code.:

Synonyms:{Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine

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Chemical Property of {Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine

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Technology Process of {Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine

There total 1 articles about {Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 871-84-1
1,7-Octadiyne

: 13686-66-3
N,N-diethylaminodimethylsilane

: 122214-22-6
{Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-silanyl}-diethyl-amine

: 122214-23-7
{Dimethyl-[2-methylene-cyclohex-(E)-ylidenemethyl]-silanyl}-diethyl-amine

Guidance literature:: With diisobutylaluminium hydride; bis(acetylacetonate)nickel(II); In benzene; at 50 ℃; for 6h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00198a100

Reference yield:

: 122214-22-6,122214-23-7
{Dimethyl-[2-methylene-cyclohex-(E)-ylidenemethyl]-silanyl}-diethyl-amine

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 122214-14-6
Dimethyl-[2-methylene-cyclohex-(Z)-ylidenemethyl]-((E)-3-phenyl-allyloxy)-silane

Guidance literature:: In diethyl ether; for 10h; Ambient temperature;
DOI:10.1021/ja00198a100

Reference yield:

: 122214-22-6,122214-23-7
{Dimethyl-[2-methylene-cyclohex-(E)-ylidenemethyl]-silanyl}-diethyl-amine

: 122214-16-8
(1S,2R,3R)-2-Hydroxymethyl-3-phenyl-1,2,3,4,5,6,7,8-octahydro-naphthalen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 10 h / Ambient temperature

2: xylene / 40 h / Heating

3: 30percent H₂O₂, KF, KHCO₃ / tetrahydrofuran; methanol / 18 h / 50 °C

With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; xylene;
DOI:10.1021/ja00198a100