N¹-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide

Base Information

• Chemical Name: N¹-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide
• CAS No.: 265103-45-5
• Molecular Formula: C₁₆H₂₂N₈O₂S
• Molecular Weight: 390.469

Synonyms:N¹-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide

Chemical Property of N¹-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide

Chemical Property:

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Technology Process of N¹-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide

There total 5 articles about N¹-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

α-Acetylamino-β,β-dimethyl-β-propiothiolactone (108865-98-1) + 2-(4-aminophenylamino)-4,6-diamino-1,3,5-triazine (57230-74-7) → N1-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide (265103-45-5)

Guidance literature:

In N,N-dimethyl-formamide; at 25 ℃; for 18h;

DOI:10.1016/S0040-4020(01)00694-9

Reference yield:

N-acetyl-p-phenylenediamine (122-80-5) → N1-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide (265103-45-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / NaOH / H₂O / 4.5 h / Heating

2: 37 percent / HCl / H₂O / 1.5 h / Heating

3: 30 percent / dimethylformamide / 18 h / 25 °C

With hydrogenchloride; sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)00694-9

Reference yield:

2-(4-acetylaminophenyl)-4,6-diamino-1,3,5-triazine (57230-73-6) → N1-4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl-2-(acetylamino)-3-methyl-3-sulfanylbutanamide (265103-45-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 37 percent / HCl / H₂O / 1.5 h / Heating

2: 30 percent / dimethylformamide / 18 h / 25 °C

With hydrogenchloride; In water; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)00694-9

upstream raw materials:

α-Acetylamino-β,β-dimethyl-β-propiothiolactone

2-(4-aminophenylamino)-4,6-diamino-1,3,5-triazine

DL-Penicillamin

N-acetyl-p-phenylenediamine

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