5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione

Base Information

• Chemical Name: 5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione
• CAS No.: 1071781-21-9
• Molecular Formula: C₁₄H₁₅N₅O₂S₂
• Molecular Weight: 349.437

Synonyms:5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione

Chemical Property of 5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione

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Technology Process of 5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione

There total 1 articles about 5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

carbon disulfide (75-15-0,12122-00-8) + 3,3′-(phenylazanediyl)dipropanehydrazide (56329-74-9) → 5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione (1071781-21-9)

Guidance literature:

carbon disulfide; With potassium hydroxide; In ethanol; at 20 ℃; for 0.25h;

3,3′-(phenylazanediyl)dipropanehydrazide; In ethanol; for 24h; Heating;

With hydrogenchloride; In water; pH=3 - 4; Further stages.;

DOI:10.1007/s10593-007-0176-9

Reference yield: 66.0%

5-(2-{[2-(2-thioxo-2,3-dihydro-1,3,4-oxadiazol-5-yl)ethyl]anilino}ethyl)-2,3-dihydro-1,3,4-oxadiazole-2-thione (1071781-21-9) → 4-amino-3-(2-{[2-(4-amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-yl)ethyl]anilino}ethyl)-4,5-dihydro-1H-1,2,4-triazole-5-thione (1071781-23-1)

Guidance literature:

With hydrazine; In 1,4-dioxane; for 10h; Heating;

DOI:10.1007/s10593-007-0176-9

upstream raw materials:

carbon disulfide

3,3′-(phenylazanediyl)dipropanehydrazide

Downstream raw materials:

4-amino-3-(2-{[2-(4-amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-yl)ethyl]anilino}ethyl)-4,5-dihydro-1H-1,2,4-triazole-5-thione

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