tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate

Base Information

Chemical Name:tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate
CAS No.:1332650-72-2
Molecular Formula:C₂₆H₃₉N₅O₅
Molecular Weight:501.626
Hs Code.:

Synonyms:tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate

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Chemical Property of tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate

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Technology Process of tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate

There total 2 articles about tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1332650-54-0
C₁₅H₂₈N₂O₄S

: 18934-57-1,91384-06-4
N-acetyl-L-phenylalaninehydrazide

: 1332650-72-2
tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate

Guidance literature:: With silver benzoate; acetic acid; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2011.07.011

Reference yield:

: 3618-96-0
(S)-N-acetylphenylalanine

: 1332650-72-2
tert-butyl (S)-1-(4-((ethoxycarbonyl)methyl)-5-((S)-1-acetamido-2-phenylethyl)-4H-1,2,4-triazol-3-yl)pentylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 20 °C

2: silver benzoate; acetic acid / dichloromethane / 6 h / 20 °C

With silver benzoate; hydrazine hydrate; acetic acid; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.07.011