Technology Process of C15H14BrNO3
There total 5 articles about C15H14BrNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron dimethyl-trifluoro sulphide;
In
dichloromethane; 1,2-dichloro-ethane;
Reflux;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.12.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere
2: zinc dibromide / toluene / 24 h / Reflux; Inert atmosphere; Molecular sieve
3: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere
With
Jones reagent; boron dimethyl-trifluoro sulphide; zinc dibromide;
In
dichloromethane; 1,2-dichloro-ethane; acetone; toluene;
2: Bohlmann-Rahtz reaction;
DOI:10.1016/j.bmcl.2011.12.015
- Guidance literature:
-
Multi-step reaction with 2 steps
1: zinc dibromide / toluene / 24 h / Reflux; Inert atmosphere; Molecular sieve
2: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere
With
boron dimethyl-trifluoro sulphide; zinc dibromide;
In
dichloromethane; 1,2-dichloro-ethane; toluene;
1: Bohlmann-Rahtz reaction;
DOI:10.1016/j.bmcl.2011.12.015