((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

Base Information

Chemical Name:((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3
CAS No.:400887-93-6
Molecular Formula:C₄₁H₅₁Al₂NO₃
Molecular Weight:659.824
Hs Code.:

((C<sub>4</sub>H<sub>9</sub>)CH<sub>3</sub>C<sub>6</sub>H<sub>2</sub>O)2CHOC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)CHNCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>Al<sub>2</sub>(CH<sub>3</sub>)3

Synonyms:((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

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Chemical Property of ((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

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Technology Process of ((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

There total 1 articles about ((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: ((C₄H₉)CH₃C₆H₂OH)2CHOHC₆H₂(CH₃)CHNCH₂C₆H₅

: 75-24-1
trimethylaluminum

: 400887-93-6
((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

Guidance literature:: In toluene; a soln. of (CH3)3Al in toluene was added to a cooled (0°C) soln. of tris(hydroxyphenol)-compound in toluene, the mixt. was held at 0°C for 1 h, allowed to warm to room temp. for 4 h (N2); the solvent was removed in vac., the residue was dissolved in pentane, stirred for 1 h, ppt. was filtered off, dried; elem. anal.;
DOI:10.1021/om010773b

Reference yield: 58.0%

: 400887-93-6
((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 400887-97-0
((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3OS(CH₃)2

Guidance literature:: In dichloromethane; a soln. of DMSO in CH2Cl2 was added to a soln. of complex in CH2Cl2, themixt. was stirred overnight (N2); reduced in vol., stored at -30°C for several days, crystals were washed with cold pentane, dried; elem. anal.;
DOI:10.1021/om010773b

Reference yield: 52.0%

: 400887-93-6
((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNCH₂C₆H₅Al₂(CH₃)3

: 400887-98-1
((C₄H₉)CH₃C₆H₂O)2CHOC₆H₂(CH₃)CHNHCH₂C₆H₅Al(CH₃)

Guidance literature:: With cyclohexanone or cyclopentanone; In dichloromethane; byproducts: 2-cyclohexylidenecyclohexanone; a soln. of ketone in CH2Cl2 was added to a soln. of complex in CH2Cl2 at-30°C, allowed to stir at room temp. for 12 h (N2); reduced in vol., stored at -30°, the solid was dried; elem. anal.;
DOI:10.1021/om010773b