(neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum

Base Information

• Chemical Name: (neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum
• CAS No.: 126949-72-2
• Molecular Formula: C₄₁H₆₁MoNO₂
• Molecular Weight: 695.881
• Mol file: 126949-72-2.mol

Synonyms:(neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum

Chemical Property of (neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum

Chemical Property:

Purity/Quality:

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Technology Process of (neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum

There total 1 articles about (neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

lithium 2,6-diisopropylphenolate (72727-49-2) + (neopentylidyne)(2,6-diisopropylphenylamido)(1,2-dimethoxyethane)molybdenum(Cl)2 → (neopentylidyne)(2,6-diisopropylphenylamido)(2,6-diisopropylphenoxide)2 molybdenum (126949-72-2)

Guidance literature:

In diethyl ether; byproducts: LiCl; solid complex is added slowly to a stirred ether soln. of LiOC6H3(iPr)2 at -30°C, LiCl precipitates as the react. is allowed to warm to room temp. over 90 min.; solvent is removed in vac., residue is extracted with pentane, extract is filtered, evapn. to solid,, recrystn. from pentane at -40°C, elem. anal.;

DOI:10.1021/ja00166a023

upstream raw materials:

lithium 2,6-diisopropylphenolate

Refernces