C₄₇H₅₂O₁₀S

Base Information

Chemical Name:C₄₇H₅₂O₁₀S
CAS No.:482626-52-8
Molecular Formula:C₄₇H₅₂O₁₀S
Molecular Weight:808.99
Hs Code.:

C<sub>47</sub>H<sub>52</sub>O<sub>10</sub>S

Synonyms:C₄₇H₅₂O₁₀S

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Chemical Property of C₄₇H₅₂O₁₀S

Chemical Property:

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Technology Process of C₄₇H₅₂O₁₀S

There total 16 articles about C₄₇H₅₂O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-59-9
p-toluenesulfonyl chloride

: 482626-51-7
C₄₀H₄₆O₈

: 482626-52-8
C₄₇H₅₂O₁₀S

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ja0279646

Reference yield:

: 482626-35-7
(2R,3S,4S,5S)-5-Benzyloxymethoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-heptane-1,3-diol

: 482626-52-8
C₄₇H₅₂O₁₀S

Guidance literature:: Multi-step reaction with 11 steps

1: 100 percent / imidazole / CH₂Cl₂ / 1 h / 0 °C

2: 93 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

3: 93 percent / tetrabutylammonium fluoride / tetrahydrofuran / 8 h / 20 °C

4: 96 percent / triethylamine; sulfur trioxide pyridine complex / dimethylsulfoxide; CH₂Cl₂ / 3 h / 20 °C

5: 99 percent / MgBr₂*Et₂O / CH₂Cl₂ / 3 h / 20 °C

6: osmium tetroxide; NMO / acetone; H₂O / 1.5 h / 20 °C

7: NaIO₄ / acetone; H₂O / 0.5 h / 20 °C

8: 3.24 g / NaBH₄ / ethanol / 0.5 h / 20 °C

9: 93 percent / pyridine; DMAP / CH₂Cl₂ / 24 h / 20 °C

10: 88 percent / CAN / acetonitrile; H₂O / 0.5 h / 20 °C

11: 99 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; triethylamine; magnesium bromide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja0279646

Reference yield:

: 374752-81-5
(2S,3R,4R,5S)-3-Benzyloxy-5-benzyloxymethoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-heptanal

: 482626-52-8
C₄₇H₅₂O₁₀S

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / MgBr₂*Et₂O / CH₂Cl₂ / 3 h / 20 °C

2: osmium tetroxide; NMO / acetone; H₂O / 1.5 h / 20 °C

3: NaIO₄ / acetone; H₂O / 0.5 h / 20 °C

4: 3.24 g / NaBH₄ / ethanol / 0.5 h / 20 °C

5: 93 percent / pyridine; DMAP / CH₂Cl₂ / 24 h / 20 °C

6: 88 percent / CAN / acetonitrile; H₂O / 0.5 h / 20 °C

7: 99 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; triethylamine; magnesium bromide; In ethanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/ja0279646