2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

Base Information

Chemical Name:2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine
CAS No.:72163-39-4
Molecular Formula:C₃₀H₃₂N₄O₁₁
Molecular Weight:624.604
Hs Code.:

2',3'-dideoxy-2',3'-<N-(benzyloxycarbonyl)epimo>-3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

Synonyms:2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

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Technology Process of 2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

There total 1 articles about 2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 66787-84-6
O⁴-[6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(toluene-4-sulfonyl)-α-D-2,6-dideoxy-glucopyranosyl]-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-1D-2-deoxy-streptamine

: 72163-39-4
2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 24h;
DOI:10.1021/jm00175a009

Reference yield: 65.0%

: 72163-39-4
2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

: 72163-40-7
2',3'-dideoxy-2',3'-epimo-3-N-(benzyloxycarbonyl)neamine

Guidance literature:: With barium hydroxide octahydrate; In 1,4-dioxane; at 60 ℃; for 7h;
DOI:10.1021/jm00175a009

Reference yield:

: 72163-39-4
2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylenamine

: 57785-94-1
2',3'-epiminoneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / barium hydroxide octahydrate / dioxane / 7 h / 60 °C

2: Na / liquid ammonia / 2 h / -70 °C

With barium hydroxide octahydrate; sodium; In 1,4-dioxane; ammonia;
DOI:10.1021/jm00175a009