[(N,N,N',N'-tetramethylethylenediamine)Pt(CH₃)(Et₂O)][(3,5-(CF₃)2C₆H₃)4B]

Base Information

• Chemical Name: [(N,N,N',N'-tetramethylethylenediamine)Pt(CH₃)(Et₂O)][(3,5-(CF₃)2C₆H₃)4B]
• CAS No.: 185849-12-1
• Molecular Formula: C₁₁H₂₉N₂OPt*C₃₂H₁₂BF₂₄
• Molecular Weight: 1263.66

Synonyms:[(N,N,N',N'-tetramethylethylenediamine)Pt(CH₃)(Et₂O)][(3,5-(CF₃)2C₆H₃)4B]

Chemical Property of [(N,N,N',N'-tetramethylethylenediamine)Pt(CH₃)(Et₂O)][(3,5-(CF₃)2C₆H₃)4B]

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Technology Process of [(N,N,N',N'-tetramethylethylenediamine)Pt(CH₃)(Et₂O)][(3,5-(CF₃)2C₆H₃)4B]

There total 2 articles about [(N,N,N',N'-tetramethylethylenediamine)Pt(CH₃)(Et₂O)][(3,5-(CF₃)2C₆H₃)4B] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

Brookhart's acid + dichloro(N,N,N`,N`-tetramethylethylenediamine)platinum(II) (18957-89-6) → [(N,N,N',N'-tetramethylethylenediamine)Pt(CH3)(Et2O)][(3,5-(CF3)2C6H3)4B] (185849-12-1)

Guidance literature:

In diethyl ether; byproducts: CH4; addn. of 1 equiv. B-compd. to Pt-complex at -78°C, warming; immediate solvent removal (vac.), dissoln. in cold Et2O, pptn. on addn. of petroleum ether, decantation, drying (vac.); elem. anal.;

Reference yield:

dimethyl(N,N,N',N',-tetramethylethanediamine)platinum + H[B(C8H3F6)4]*99diethyl ether → [(N,N,N',N'-tetramethylethylenediamine)Pt(CH3)(Et2O)][(3,5-(CF3)2C6H3)4B] (185849-12-1)

Guidance literature:

In diethyl ether; -70°C; elem. anal.;

DOI:10.1021/ja9620595

Reference yield: 78.0%

[(N,N,N',N'-tetramethylethylenediamine)Pt(CH3)(Et2O)][(3,5-(CF3)2C6H3)4B] (185849-12-1) → [(N,N,N',N'-tetramethylethylenediamine)Pt(=C(CH3)(OCH2CH3))(H)][(3,5-(CF3)2C6H3)4B]

Guidance literature:

In diethyl ether; byproducts: CH4; inert atmosphere; stirring at room temp. for 1 week; concn., addn. of petroleum ether, pptn. on concn. (vac.); elem. anal.;

upstream raw materials:

dichloro(N,N,N`,N`-tetramethylethylenediamine)platinum(II)

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