biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester

Base Information

• Chemical Name: biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester
• CAS No.: 412932-17-3
• Molecular Formula: C₁₉H₁₉NO₂
• Molecular Weight: 293.365
• Mol file: 412932-17-3.mol

Synonyms:biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester

Chemical Property of biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester

There total 1 articles about biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-biphenyl isocyanate (92-95-5) + Cyclohex-2-enol (822-67-3) → biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester (412932-17-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/ja012124x

Reference yield: 68.0%

biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester (412932-17-3) → (3aR,7aS)-3-Biphenyl-4-yl-hexahydro-benzooxazol-2-one

Guidance literature:

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; at 90 ℃; for 24h;

DOI:10.1021/ja012126h

Reference yield: 20.0%

biphenyl-4-yl-carbamic acid cyclohex-2-enyl ester (412932-17-3) → (3,6-dioxo-4-phenyl-cyclohexa-1,4-dienyl)-carbamic acid cyclohex-2-enyl ester + (2aR,5aS,10cS)-8-Phenyl-2a,3,4,5,5a,10c-hexahydro-2,6-dioxa-10b-aza-aceanthrylen-1-one

Guidance literature:

With water; Dess-Martin periodane; In dichloromethane; at 23 ℃; for 63h;

DOI:10.1021/ja012124x

upstream raw materials:

4-biphenyl isocyanate

Cyclohex-2-enol