kahalalide B

Base Information

• Chemical Name: kahalalide B
• CAS No.: 180714-95-8
• Molecular Formula: C₄₅H₆₃N₇O₁₁
• Molecular Weight: 878.036
• Mol file: 180714-95-8.mol

Synonyms:kahalalide B

Chemical Property of kahalalide B

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of kahalalide B

There total 3 articles about kahalalide B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C52H71N7O11S (1227413-82-2) → kahalalide B (180714-95-8)

Guidance literature:

With 1H-imidazole; In acetonitrile; at 20 ℃; for 24h;

DOI:10.1021/ol100596p

Reference yield: 65.0%

C59H75N7O11 → kahalalide B (180714-95-8)

Guidance literature:

With hydrogenchloride; palladium on activated carbon; hydrogen; acetic acid; In methanol; for 12h; under 10343.2 Torr;

DOI:10.1039/d0cc07747j

Reference yield:

C59H79N7O11S → kahalalide B (180714-95-8)

Guidance literature:

Multi-step reaction with 2 steps

1: silver carbonate / acetonitrile; dichloromethane / 96 h / 20 °C

2: acetic acid; hydrogenchloride; palladium on activated carbon; hydrogen / methanol / 12 h / 10343.2 Torr

With hydrogenchloride; palladium on activated carbon; hydrogen; acetic acid; silver carbonate; In methanol; dichloromethane; acetonitrile;

DOI:10.1039/d0cc07747j

upstream raw materials:

C₅₂H₇₁N₇O₁₁S