(4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Base Information

Chemical Name:(4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline
CAS No.:1269604-13-8
Molecular Formula:C₂₁H₂₃N₃O₄
Molecular Weight:381.431
Hs Code.:

Synonyms:(4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Suppliers and Price of (4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

There total 3 articles about (4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R)-N⁽⁴⁾-benzyloxycarbonyl-1,2,4-triaminobutane dihydrochloride

: 79944-55-1
ethyl (1,4-benzodioxan-2-yl)imidoate hydrochloride

: 1269604-13-8
(4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Guidance literature:: With triethylamine; In ethanol; for 4h; Reflux;
DOI:10.1016/j.bmc.2010.11.039

Reference yield:

: 1008-92-0
2-cyano-1,4-benzodioxane

: 1269604-13-8
(4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / diethyl ether / 72 h / 4 °C

2: triethylamine / ethanol / 4 h / Reflux

With hydrogenchloride; triethylamine; In diethyl ether; ethanol;
DOI:10.1016/j.bmc.2010.11.039

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 1269604-13-8
(4R)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-(2,3-dihydro-1,4-benzodioxan-2-yl)imidazoline

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 18 h / Reflux

2: hydrogenchloride / diethyl ether / 72 h / 4 °C

3: triethylamine / ethanol / 4 h / Reflux

With hydrogenchloride; triethylamine; In diethyl ether; ethanol; acetone;
DOI:10.1016/j.bmc.2010.11.039