(4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine

Base Information

Chemical Name:(4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine
CAS No.:1051394-22-9
Molecular Formula:C₁₆H₂₁N₃O₈S
Molecular Weight:415.424
Hs Code.:

Synonyms:(4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine

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Chemical Property of (4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine

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Technology Process of (4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine

There total 2 articles about (4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1051394-18-3
1-tert-butyl 2-methyl (2S,4R)-4-{[(2-nitrophenyl)sulfonyl]amino}pyrrolidine-1,2-dicarboxylate

: 1051394-22-9
(4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine

Guidance literature:: 1-tert-butyl 2-methyl (2S,4R)-4-{[(2-nitrophenyl)sulfonyl]amino}pyrrolidine-1,2-dicarboxylate; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 4h;

With citric acid; In dichloromethane; water; at 20 ℃;

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 121148-00-3,1018667-18-9
1-(1,1-dimethylethyl) 2-methyl (2S,4R)-4-amino-1,2-pyrrolidinedicarboxylate

: 1051394-22-9
(4R)-1-(tert-butoxycarbonyl)-4-{[(2-nitrophenyl)sulfonyl]amino}-L-proiine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C

2.1: methanol; lithium hydroxide; water / tetrahydrofuran / 4 h / 20 °C

2.2: 20 °C

With methanol; lithium hydroxide; water; triethylamine; In tetrahydrofuran; dichloromethane;