bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

Base Information

Chemical Name:bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane
CAS No.:75425-89-7
Molecular Formula:C₁₇H₂₃P₃S₃
Molecular Weight:416.489
Hs Code.:

Synonyms:bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

Suppliers and Price of bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

There total 2 articles about bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 75425-90-0
(dimethylphosphino)(dimethylthiophosphoryl)(diphenylthiophosphoryl)methane

: 75425-89-7
bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

Guidance literature:: With sulfur; In toluene; for 3h; Heating;

Reference yield:

: 38055-42-4
C₁₅H₁₈P₂S₂

: 75425-89-7
bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) THF, -78 deg C; 2.) 9 h

2: 77 percent / S / toluene / 3 h / Heating

With sulfur; In toluene;

Reference yield: 93.0%

: 75425-89-7
bis(dimethylthiophosphoryl)diphenylthiophosphorylmethane

: 7790-80-9
cadmium(II) iodide

: 97391-08-7
[(bis(dimethylthiophosphinoyl)(diphenylthiophosphinoyl)methanido)iodocadmium(II)]

Guidance literature:: With N(CH₂CH₃)3; In tetrahydrofuran; ethanol; (under N2); dropwise addn. of CdI2 in ethanol to the ligand in THF and NEt3 with rapid stirring, stirring overnight; removal of solvents by evapn., ppt. is washed, dried in vac., elem. anal.;