C₂₁H₂₂O

Base Information

Chemical Name:C₂₁H₂₂O
CAS No.:180308-62-7
Molecular Formula:C₂₁H₂₂O
Molecular Weight:290.405
Hs Code.:

Synonyms:C₂₁H₂₂O

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Chemical Property of C₂₁H₂₂O

Chemical Property:

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Technology Process of C₂₁H₂₂O

There total 1 articles about C₂₁H₂₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 768-48-9
4-acetoxy-cyclopentenone

: (R)-3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-indene

: 180308-62-7
C₂₁H₂₂O

Guidance literature:: zinc chloride diethyl ether; In dichloromethane; for 24h; under 4875390 Torr;

Reference yield: 88.0%

: 57218-61-8
allyl methyl malonate

: 180308-62-7
C₂₁H₂₂O

: C₂₈H₃₂O₅

Guidance literature:: With 18-crown-6 ether; potassium carbonate; for 168h; Ambient temperature;

Reference yield:

: 180308-62-7
C₂₁H₂₂O

: 1211-29-6
Methyl jasmonate

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / K₂CO₃, 18-crown-6 / 168 h / Ambient temperature

2: 60 percent / LDA / tetrahydrofuran / 1.) -78 deg C to -40 deg C, 2.) -78 deg C

3: 65 percent / HCO₂H, NEt₃ / PPh₃/Pd(OAc)2 / dioxane / 72 h / Heating

4: 83 percent / NaBH₄ / tetrahydrofuran; methanol / 1.) 0 deg C to r.t., 2.) 40 deg C, 2 d

5: 98 percent / 2 h / 405 °C / 0.01 Torr

6: 72 percent / H₂ / 10percent Pd/CaCO₃ / methanol / 12 h / Ambient temperature

7: PCC, sodium acetate / CH₂Cl₂ / 19 h

With sodium tetrahydroborate; formic acid; 18-crown-6 ether; hydrogen; sodium acetate; potassium carbonate; triethylamine; pyridinium chlorochromate; lithium diisopropyl amide; palladium diacetate; Lindlar's catalyst; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;