1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Base Information

• Chemical Name: 1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine
• CAS No.: 77563-30-5
• Molecular Formula: C₂₃H₂₈N₄O₂S
• Molecular Weight: 424.567

Synonyms:1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Chemical Property of 1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Chemical Property:

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Technology Process of 1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

There total 2 articles about 1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.7%

2-methoxybenzo[d]thiazol-6-amine (77563-27-0) + 1-(2-bromopropionyl)-4-phenethylpiperazine (77563-21-4) → 1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine (77563-30-5)

Guidance literature:

With potassium carbonate; In ethanol; for 6h; Heating;

DOI:10.1248/cpb.28.3315

Reference yield:

4-(phenethyl)piperazine (5321-49-3) → 1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine (77563-30-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 16 g / benzene / 2 h / 5 °C

2: 40.7 percent / K₂CO₃ / ethanol / 6 h / Heating

With potassium carbonate; In ethanol; benzene;

DOI:10.1248/cpb.28.3315

Reference yield: 95.7%

1-<2-(2-methoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine (77563-30-5) → 6-<1-methyl-2-(4-phenethylpiperazino)ethyl>-amino-2-methoxy-benzothiazole (77563-03-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 5h; Heating;

DOI:10.1248/cpb.28.3315

upstream raw materials:

2-methoxybenzo[d]thiazol-6-amine

1-(2-bromopropionyl)-4-phenethylpiperazine

4-(phenethyl)piperazine

Downstream raw materials:

6-<1-methyl-2-(4-phenethylpiperazino)ethyl>-amino-2-methoxy-benzothiazole

2-methoxy-6--propionamide>-benzothiazole

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