N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

Base Information

Chemical Name:N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide
CAS No.:943151-76-6
Molecular Formula:C₃₄H₄₄N₂O₅
Molecular Weight:560.734
Hs Code.:

Synonyms:N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

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Technology Process of N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

There total 1 articles about N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 8-(4-benzyloxyphenoxy)-1-octylamine hydrochloride

: 2900-27-8
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid

: 943151-76-6
N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jm061349l

Reference yield: 73.2%

: 943151-76-6
N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

: 943151-78-8
N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-amino-2-phenylacetamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1021/jm061349l

Reference yield:

: 943151-76-6
N-[8-(4-benzyloxyphenoxy)-1-octyl]-2-(N'-tert-butoxycarbonylamino)-2-phenylacetamide

: C₃₂H₄₃N₂O₃⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: 73.2 percent / TFA / CH₂Cl₂ / 20 °C

2: 58.1 percent / K₂CO₃ / 1,2-dimethoxy-ethane / 20 °C

With potassium carbonate; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/jm061349l