(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

Base Information

Chemical Name:(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate
CAS No.:1393803-02-5
Molecular Formula:C₂₅H₂₆N₃O*ClO₄
Molecular Weight:483.952
Hs Code.:

Synonyms:(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

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Chemical Property of (S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

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Technology Process of (S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

There total 3 articles about (S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 83053-86-5
(S)-1-(benzyloxy)-3-phenylpropan-2-amine

: 17646-51-4
5-methyl-3-phenyl-[1,3,4]oxadiazol-3-ium perchlorate

: 1393803-02-5
(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

Guidance literature:: With acetic acid; at 110 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.06.002

Reference yield:

: 3182-95-4
L-Phenylalaninol

: 1393803-02-5
(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

2: acetic acid / 2 h / 110 °C / Inert atmosphere

With sodium hydride; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2012.06.002

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1393803-02-5
(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

2: sodium hydride / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

3: acetic acid / 2 h / 110 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2012.06.002