N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide

Base Information

Chemical Name:N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide
CAS No.:1193723-98-6
Molecular Formula:C₂₃H₂₈N₄O₅
Molecular Weight:440.499
Hs Code.:

N<sub>3</sub>,N<sub>3</sub>-diethyl-N<sub>1</sub>-(2,4-dimethoxybenzyl)-N<sub>1</sub>-(3-methoxyphenyl)-2-diazomalonamide

Synonyms:N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide

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Technology Process of N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide

There total 1 articles about N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1193723-96-4
2-diazo-3-(diethylamino)-3-oxopropanoyl chloride

: 1020936-75-7
(2,4-dimethoxybenzyl)-(3-methoxyphenyl)amine

: 1193723-98-6
N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.08.006

Reference yield: 88.0%

: 1193723-98-6
N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1193724-03-6
N,N-diethyl-1-N-(2,4-dimethoxybenzyl)-6-methoxy-2-(triisopropylsilyloxy)-1H-indole-3-carboxamide

Guidance literature:: N₃,N₃-diethyl-N₁-(2,4-dimethoxybenzyl)-N₁-(3-methoxyphenyl)-2-diazomalonamide; With tetrakis(μ-trifluoroacetamidato)dirhodium(II); In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

triisopropylsilyl trifluoromethanesulfonate; With triethylamine; In dichloromethane; at 0 ℃; for 0.25h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.08.006