(1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate

Base Information

• Chemical Name: (1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate
• CAS No.: 1039433-83-4
• Molecular Formula: C₃₇H₄₀FNO₈
• Molecular Weight: 645.725

Synonyms:(1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate

Chemical Property of (1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate

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Technology Process of (1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate

There total 1 articles about (1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate (1039433-82-3) + tri-n-butyl(vinyl)tin (7486-35-3) → (1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate (1039433-83-4)

Guidance literature:

With lithium chloride; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 90 ℃; for 4h;

Reference yield:

(1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-vinylphenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate (1039433-83-4) → (1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-1-[4-(1,2-dihydroxyethyl)phenyl]-4-oxoazetidin-3-yl]-1-(4-fluorophenyl)propyl acetate (1039433-84-5)

Guidance literature:

With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In acetone; at 20 ℃; for 3h;

upstream raw materials:

(1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-4-oxo-1-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)azetidin-3-yl]-1-(4-fluorophenyl)propyl acetate

tri-n-butyl(vinyl)tin

Downstream raw materials:

(1S)-3-[(2S,3R)-2-(4-{4-(acetyloxy)-3-[(acetyloxy)methyl]-3-hydroxybutyl}phenyl)-1-[4-(1,2-dihydroxyethyl)phenyl]-4-oxoazetidin-3-yl]-1-(4-fluorophenyl)propyl acetate

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