4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Base Information

Chemical Name:4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone
CAS No.:1366133-63-2
Molecular Formula:C₁₇H₉Cl₂FN₂O₃
Molecular Weight:379.174
Hs Code.:

Synonyms:4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Suppliers and Price of 4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

There total 2 articles about 4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1366133-70-1
4-acetyl-3-(3-chloro-4-fluorophenyl)sydnone

: 104-88-1
4-chlorobenzaldehyde

: 1366133-63-2
4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Guidance literature:: With sodium hydroxide; In ethanol; water; at 5 - 10 ℃; for 0.333333h; Sonication;
DOI:10.14233/ajchem.2015.18864

Reference yield:

: 68657-50-1
3-(3-chloro-4-fluorophenyl)sydnone

: 1366133-63-2
4-[1-oxo-3-(4-chlorophenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentoxide

2: sodium hydroxide / ethanol; water / 1 h / 5 - 10 °C

With phosphorus pentoxide; sodium hydroxide; In ethanol; water; 2: Claisen-Schmidt reaction;
DOI:10.3109/14756366.2011.586345