3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

Base Information

Chemical Name:3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid
CAS No.:1263403-94-6
Molecular Formula:C₂₁H₁₉N₃O₆
Molecular Weight:409.398
Hs Code.:

Synonyms:3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

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Chemical Property of 3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

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Technology Process of 3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

There total 14 articles about 3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1263403-95-7
methyl 3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxopyrrolidin-3-yloxy)benzoate

: 1263403-94-6
3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

Guidance literature:: methyl 3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxopyrrolidin-3-yloxy)benzoate; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With hydrogenchloride; In water;

Reference yield:

: 33693-57-1
3-bromo-1-methyl-pyrrolidin-2-one

: 1263403-94-6
3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: N,N-dimethylglycine hydrochoride / copper(II) iodide / 1,4-dioxane / 24 h / Inert atmosphere; Reflux

3: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

With water; N,N-dimethylglycine hydrochoride; potassium carbonate; sodium hydroxide; copper(II) iodide; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1263403-94-6
3-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenoxy)-5-(1-methyl-2-oxo pyrrolidin-3-yloxy)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: N,N-dimethylglycine hydrochoride / copper(II) iodide / 1,4-dioxane / 24 h / Inert atmosphere; Reflux

3: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

With water; N,N-dimethylglycine hydrochoride; potassium carbonate; sodium hydroxide; copper(II) iodide; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;