2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol

Base Information

• Chemical Name: 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol
• CAS No.: 1206111-55-8
• Molecular Formula: C₃₀H₄₆N₄O₆Si
• Molecular Weight: 586.804

Synonyms:2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol

Chemical Property of 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol

There total 2 articles about 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol (1206111-51-4) → 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol (1206111-55-8)

Guidance literature:

With hydrogen azide; di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 20 ℃; for 16.5h;

DOI:10.1002/ejoc.200900971

Reference yield:

C31H49NO9SSi (1206111-87-6) → 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol (1206111-55-8)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; for 17h;

DOI:10.1002/ejoc.200900971

Reference yield:

2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol (1206111-55-8) → 2-azido-3-O-benzyl-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol (1206111-54-7)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1002/ejoc.200900971

upstream raw materials:

3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

C₃₁H₄₉NO₉SSi

Downstream raw materials:

2-azido-3-O-benzyl-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1206111-55-8 2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-2,4-deoxy-5-O-(4-methoxyphenyl)-L-ribitol

Send

Send

Metric Ton KG G Pound L ML

Send

Send