Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

Base Information

Chemical Name:Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside
CAS No.:141263-05-0
Molecular Formula:C₅₄H₅₈O₁₀
Molecular Weight:867.049
Hs Code.:

Synonyms:Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

Suppliers and Price of Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

There total 9 articles about Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 141263-04-9
Benzyl 3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-2,4-di-O-benzyl-α-L-rhamnopyranoside

: 141263-05-0
Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: With sodium methylate; In methanol; pH 10, overnight;
DOI:10.1016/S0008-6215(00)90498-1

Reference yield:

: 20701-61-5
ethyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 141263-05-0
Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / NaH / dimethylformamide / 1 h / 0 °C

2: 1) borane-trimethylamine complex, molecular sieves (4 Angstroem), 2) AlCl₃ / 1) THF, 1 h, 2) 0 deg C, 3 h

3: 99 percent / pyridine / 16 h / Ambient temperature

4: 57 percent / molecular sieves (4 Angstroem), methyl triflate / diethyl ether / 18 h

5: 98 percent / NaOMe / methanol / pH 10, overnight

With pyridine; aluminium trichloride; trimethylamine-borane; 4 A molecular sieve; sodium methylate; sodium hydride; methyl trifluoromethanesulfonate; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90498-1

Reference yield:

: 62774-11-2
Benzyl 2,4-di-O-benzyl-α-L-rhamnopyranoside

: 141263-05-0
Benzyl 2,4-di-O-benzyl-3-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / molecular sieves (4 Angstroem), methyl triflate / diethyl ether / 18 h

2: 98 percent / NaOMe / methanol / pH 10, overnight

With 4 A molecular sieve; sodium methylate; methyl trifluoromethanesulfonate; In methanol; diethyl ether;
DOI:10.1016/S0008-6215(00)90498-1