[(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

Base Information

Chemical Name:[(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol
CAS No.:135191-51-4
Molecular Formula:C₂₃H₃₈O₈
Molecular Weight:442.55
Hs Code.:

Synonyms:[(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

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Chemical Property of [(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

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Technology Process of [(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

There total 8 articles about [(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: (1R,2R,4R)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentanecarboxylic acid dimethylamide

: 135191-51-4
[(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

: 135191-50-3
(1R,2R,4R)-2-<(S)-1-<(2-methoxyethoxy)methoxy>-2-(phenylmethoxy)ethyl>-4-<(2-methoxyethoxy)methoxy>cyclopentanecarboxaldehyde

: 135191-50-3,135269-24-8
(1S,2R,4R)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentanecarbaldehyde

Guidance literature:: With n-butyllithium; diisobutylaluminium hydride; In tetrahydrofuran; hexane; toluene; for 0.933333h;

Reference yield:

: 100-44-7
benzyl chloride

: 135191-51-4
[(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / NaH / dimethylsulfoxide / 1 h / Ambient temperature

2: 93 percent / O₃, pyridine / CH₂Cl₂; methanol / 0.06 h

3: 0.435 g / KMnO₄, t-butyl alcohol, ph7 phosphate buffer / H₂O / 0.92 h

4: 1.) triethylamine / 1.) THF, -40 deg C, 22 min, 2.) THF, H₂O, 2.5 h

5: 65 percent / KH / tetrahydrofuran / 13 h

6: N,N-diisopropylethylamine / CH₂Cl₂ / 23 h

7: 29 percent / n-BuLi, DIBAL / tetrahydrofuran; toluene; hexane / 0.93 h

With pyridine; potassium permanganate; n-butyllithium; ph7 phosphate buffer; potassium hydride; sodium hydride; diisobutylaluminium hydride; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; tert-butyl alcohol; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; toluene;

Reference yield:

: 135191-44-5
(2R,3R)-2-Benzyloxymethyl-3-[(S)-2-(2-methoxy-ethoxymethoxy)-6-methyl-hept-5-enyl]-oxirane

: 135191-51-4
[(1R,2R,4S)-2-[(S)-2-Benzyloxy-1-(2-methoxy-ethoxymethoxy)-ethyl]-4-(2-methoxy-ethoxymethoxy)-cyclopentyl]-methanol

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / O₃, pyridine / CH₂Cl₂; methanol / 0.06 h

2: 0.435 g / KMnO₄, t-butyl alcohol, ph7 phosphate buffer / H₂O / 0.92 h

3: 1.) triethylamine / 1.) THF, -40 deg C, 22 min, 2.) THF, H₂O, 2.5 h

4: 65 percent / KH / tetrahydrofuran / 13 h

5: N,N-diisopropylethylamine / CH₂Cl₂ / 23 h

6: 29 percent / n-BuLi, DIBAL / tetrahydrofuran; toluene; hexane / 0.93 h

With pyridine; potassium permanganate; n-butyllithium; ph7 phosphate buffer; potassium hydride; diisobutylaluminium hydride; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; tert-butyl alcohol; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene;