6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester

Base Information

• Chemical Name: 6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester
• CAS No.: 913338-76-8
• Molecular Formula: C₄₅H₆₀N₂O₇
• Molecular Weight: 740.981

Synonyms:6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester

Chemical Property of 6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester

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Technology Process of 6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester

There total 1 articles about 6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N(α)-benzyloxycarbonyl-L-lysine benzyl ester (5591-94-6) + 3β-acetoxybisnor-5-cholenic acid (1474-14-2) → 6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester (913338-76-8)

Guidance literature:

3β-acetoxybisnor-5-cholenic acid; With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 1h;

N^(α)-benzyloxycarbonyl-L-lysine benzyl ester; In N,N-dimethyl-formamide;

DOI:10.1021/jm060290f

Reference yield: 36.0%

6-[2-(3-acetoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-2-benzyloxycarbonylamino-hexanoic acid benzyl ester (913338-76-8) → 2-benzyloxycarbonylamino-6-[2-(3-hydroxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-hexanoic acid (913338-34-8)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; at 50 ℃; for 24h;

DOI:10.1021/jm060290f

upstream raw materials:

N^(α)-benzyloxycarbonyl-L-lysine benzyl ester

3β-acetoxybisnor-5-cholenic acid

Downstream raw materials:

2-benzyloxycarbonylamino-6-[2-(3-hydroxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propionylamino]-hexanoic acid

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