4-ethynylphenylmethyl 12-hydroxydodecanoate

Base Information

• Chemical Name: 4-ethynylphenylmethyl 12-hydroxydodecanoate
• CAS No.: 1256161-76-8
• Molecular Formula: C₂₁H₃₀O₃
• Molecular Weight: 330.467
• Mol file: 1256161-76-8.mol

Synonyms:4-ethynylphenylmethyl 12-hydroxydodecanoate

Chemical Property of 4-ethynylphenylmethyl 12-hydroxydodecanoate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-ethynylphenylmethyl 12-hydroxydodecanoate

There total 1 articles about 4-ethynylphenylmethyl 12-hydroxydodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-(trimethylsilylethynyl)phenylmethyl 12-[(tert-butyldimethylsilyl)oxy]dodecanoate (1256161-75-7) → 4-ethynylphenylmethyl 12-hydroxydodecanoate (1256161-76-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.833333h;

DOI:10.1002/anie.201004074

Reference yield: 87.0%

4-ethynylphenylmethyl 12-hydroxydodecanoate (1256161-76-8) + 1,2-dihydro-1,2-methanofullerene[60]-61-carboxylic acid (155116-19-1) → C83H30O4 (1256161-71-3)

Guidance literature:

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In bromobenzene; at 20 ℃;

DOI:10.1002/anie.201004074

upstream raw materials:

4-(trimethylsilylethynyl)phenylmethyl 12-[(tert-butyldimethylsilyl)oxy]dodecanoate

Downstream raw materials:

C₈₃H₃₀O₄