apigenin-7-O-β-D-tetra-O-acetylgalactoside

Base Information

Chemical Name:apigenin-7-O-β-D-tetra-O-acetylgalactoside
CAS No.:1389307-04-3
Molecular Formula:C₂₉H₂₈O₁₄
Molecular Weight:600.533
Hs Code.:

Synonyms:apigenin-7-O-β-D-tetra-O-acetylgalactoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of apigenin-7-O-β-D-tetra-O-acetylgalactoside

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Technology Process of apigenin-7-O-β-D-tetra-O-acetylgalactoside

There total 5 articles about apigenin-7-O-β-D-tetra-O-acetylgalactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 23598-19-8
4'-O-benzylapigenin-7-O-β-D-tetra-O-acetylgalactoside

: 1389307-04-3
apigenin-7-O-β-D-tetra-O-acetylgalactoside

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; ethyl acetate; at 20 ℃;
DOI:10.1016/j.carres.2012.05.013

Reference yield:

: 52309-82-7
4′-O-benzylapigenin

: 1389307-04-3
apigenin-7-O-β-D-tetra-O-acetylgalactoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; potassium carbonate / chloroform / 12 h / 45 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / methanol; ethyl acetate / 20 °C

With 5%-palladium/activated carbon; tetrabutylammomium bromide; hydrogen; potassium carbonate; In methanol; chloroform; ethyl acetate;
DOI:10.1016/j.carres.2012.05.013

Reference yield:

: C₃₄H₃₆O₁₄

: 1389307-04-3
apigenin-7-O-β-D-tetra-O-acetylgalactoside

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / ethanol / 2 h / Reflux

2: tetrabutylammomium bromide; potassium carbonate / chloroform / 12 h / 45 °C / Inert atmosphere

3: 5%-palladium/activated carbon; hydrogen / methanol; ethyl acetate / 20 °C

With sulfuric acid; 5%-palladium/activated carbon; tetrabutylammomium bromide; hydrogen; potassium carbonate; In methanol; ethanol; chloroform; ethyl acetate;
DOI:10.1016/j.carres.2012.05.013