tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

Base Information

Chemical Name:tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate
CAS No.:1312583-91-7
Molecular Formula:C₂₀H₂₈N₂O₃S
Molecular Weight:376.52
Hs Code.:

Synonyms:tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

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Chemical Property of tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

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Technology Process of tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

There total 3 articles about tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1312583-78-0
tert-butyl (1S,2S)-1-(5-(bromomethyl)oxazol-2-yl)-2-methylbutylcarbamate

: 108-98-5
thiophenol

: 1312583-91-7
tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c1ob05390f

Reference yield:

: 1312583-85-9
tert-butyl (1S,2S)-2-methyl-1-(5-methylene-4,5-dihydrooxazol-2-yl)butylcarbamate

: 1312583-91-7
tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / chloroform / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

With bromine; potassium carbonate; In chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05390f

Reference yield:

: 1268671-02-8
tert-butyl (2S,3S)-3-methyl-1-oxo-1-(prop-2-ynylamino)pentan-2-ylcarbamate

: 1312583-91-7
tert-butyl (1S,2S)-2-methyl-1-(5-(phenylthiomethyl)oxazol-2-yl)butylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: gold(III) chloride / chloroform / 20 °C / Inert atmosphere

2: bromine / chloroform / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

With gold(III) chloride; bromine; potassium carbonate; In chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05390f