(Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)}

Base Information

• Chemical Name: (Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)}
• CAS No.: 137003-14-6
• Molecular Formula: 2C₁₆H₃₆N*C₅₂H₄₈Fe₄S₁₄
• Molecular Weight: 1830.2
• Mol file: 137003-14-6.mol

Synonyms:(Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)}

Chemical Property of (Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)}

There total 1 articles about (Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(Bu4N)2{Fe4S4(SMe)4} (50923-26-7) + 1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene (107540-22-7) + sodium thiomethoxide (5188-07-8) → (Bu4N)2{Fe4S4(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)} (137003-14-6)

Guidance literature:

In chloroform; acetonitrile; byproducts: HSCH3; (N2); stirred under dynamic vacuum for 6 h; solvent evapd.; dissolved in acetonitrile; filtered; addn. of NaSMe; stirred for 8 h; filtered; evaporated;

Reference yield: 83.0%

2-Sulfanylpyridine (2637-34-5,73018-10-7) + (Bu4N)2{Fe4S4(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(SMe)} (137003-14-6) → (Bu4N)2{Fe4S4(1,3,5-tris((4,6-dimethyl-3-mercapto-phenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(S-2-py)} (137003-16-8)

Guidance literature:

In acetonitrile; (N2); stirred under dynamic vacuum for 4 h; solvent removed; washed (toluene); dried;

upstream raw materials:

(Bu₄N)2{Fe₄S₄(SMe)4}

1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene

sodium thiomethoxide

Downstream raw materials:

(Bu₄N)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercapto-phenyl)thio)-2,4,6-tris(p-tolylthio)benzene)(S-2-py)}