N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

Base Information

Chemical Name:N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane
CAS No.:943996-05-2
Molecular Formula:C₃₀H₃₆N₆O₆
Molecular Weight:576.652
Hs Code.:

Synonyms:N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

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Technology Process of N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

There total 4 articles about N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 943996-08-5
N,N',N''-tris(2-methoxy-5-nitrobenzoyl) cis,cis-1,3,5-triaminocyclohexane

: 943996-05-2
N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; at 35 ℃; for 3h; under 3040.2 Torr;
DOI:10.1016/j.tet.2007.04.043

Reference yield:

: 943996-04-1
N,N',N''-tris(anisoyl) cis,cis-1,3,5-triaminocyclohexane

: 943996-05-2
N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / H₂SO₄; NH₄NO₃ / 0.75 h / cooling

2: 95 percent / H₂ / Pd/C / ethanol; dimethylformamide / 3 h / 35 °C / 3040.2 Torr

With ammonium nitrate; sulfuric acid; hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.04.043

Reference yield:

: 26150-46-9
cis,cis-1,3,5-triaminocyclohexane

: 943996-05-2
N,N',N''-tris(5-amino-2-methoxybenzoyl) cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / TEA / dimethylsulfoxide; tetrahydrofuran

2: 75 percent / H₂SO₄; NH₄NO₃ / 0.75 h / cooling

3: 95 percent / H₂ / Pd/C / ethanol; dimethylformamide / 3 h / 35 °C / 3040.2 Torr

With ammonium nitrate; TEA; sulfuric acid; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.04.043