Bis--phenyl-phosphin

Base Information

Chemical Name:Bis--phenyl-phosphin
CAS No.:3053-60-9
Molecular Formula:C₁₆H₂₃P
Molecular Weight:246.332
Hs Code.:

Synonyms:Bis--phenyl-phosphin

Suppliers and Price of Bis--phenyl-phosphin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis--phenyl-phosphin

Chemical Property:

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Technology Process of Bis--phenyl-phosphin

There total 2 articles about Bis--phenyl-phosphin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1119-51-3
bromopentene

: 638-21-1
phenylphosphane

: 3053-60-9
Bis--phenyl-phosphin

Guidance literature:: phenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃;

bromopentene; In tetrahydrofuran; hexane; at 0 - 20 ℃; Further stages.;
DOI:10.1039/b400156g

Reference yield:

: 1119-51-3
bromopentene

: 644-97-3
Dichlorophenylphosphine

: 3053-60-9
Bis--phenyl-phosphin

Guidance literature:: Multistep reaction; (i) Mg, Et₂O, (ii) /BRN= 508189/;
DOI:10.1139/v74-247

Reference yield: 86.0%

: 77347-62-7
[(μ-chloro)2(tetrahydrothiophene)2(pentafluorophenyl)2(platinum(II))2]

: 3053-60-9
Bis--phenyl-phosphin

: 709008-33-3
trans-[Pt(C₆F₅)Cl(P(C₆H₅)((CH₂)3CHCH₂)2)2]

Guidance literature:: In dichloromethane; (N2); charging of Schlenk flask with (Pt(μ-Cl)(C6F5)(SC4H8))2, PPh((CH2)3CHCH2)2 and CH2Cl2; stirring at room temp. for 17 h; removal of solvent by oil-pump vac.; filtration through neutral alumina using 1:1 v/v CH2Cl2-hexanes; removal of solvent by oil-pump vac., as oil; elem. anal.;
DOI:10.1039/b400156g