phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Chemical Name:phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside
CAS No.:81561-92-4
Molecular Formula:C₄₅H₅₁NO₁₂
Molecular Weight:797.899
Hs Code.:

Synonyms:phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Chemical Property of phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Technology Process of phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

There total 1 articles about phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 40555-79-1
phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside

: 33639-77-9
perbenzyl fucosyl bromide

: 81561-92-4
phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; tetrabutylammomium bromide; In dichloromethane; N,N-dimethyl-formamide; for 96h; Ambient temperature;
DOI:10.1016/S0008-6215(00)81004-6

Reference yield: 67.0%

: 81561-92-4
phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

: 81561-93-5
phenyl 2-acetamido-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; chloroform; 1.) 6 h, room temperature, 2.) 5 deg C;
DOI:10.1016/S0008-6215(00)81004-6

Reference yield:

: 81561-92-4
phenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

: 81329-65-9
phenyl 2-acetamido-2-deoxy-4-O-α-L-fucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 0.1M sodium methoxide / methanol; CHCl₃ / 1.) 6 h, room temperature, 2.) 5 deg C

2: 80 percent / hydrogen / 10percent Pd-C / acetic acid / 48 h

With hydrogen; sodium methylate; palladium on activated charcoal; In methanol; chloroform; acetic acid;
DOI:10.1016/S0008-6215(00)81004-6